Synthesis of large single-grain 1/1 approximant crystals in the Ag-In-Eu system by the self-flux method
Identifieur interne : 000692 ( Chine/Analysis ); précédent : 000691; suivant : 000693Synthesis of large single-grain 1/1 approximant crystals in the Ag-In-Eu system by the self-flux method
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Abstract
In this work, we investigate single-grain 1/1 quasicrystal approximant crystals, grown via the self-flux method, in the Ag-In-Eu system, the structure of which is similar to the 1/1 approximant in the Cd-Eu system. Due to the similarities between the Cd-RE (RE = rare earth) and Ag- In-RE systems, Ag-In-RE can be regarded as a pseudo-binary phase, in which Ag and In replace Cd. Thus, based on the binary phase diagram of Cd-Eu, the growth conditions, including the nominal composition and decanting temperatures, for single-grain Ag-In-Eu 1/1 approximant crystal growth from indium-rich melt-solution were studied. A faceted, centimeter-sized single-grain 1/1 approximant crystal was obtained and characterized using powder X-ray diffraction, scanning electron microscopy and back-reflection Laue X-ray diffraction methods. The results are promising for the synthesis of single-grain approximant crystals in other Ag-In-RE systems.
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<author><name>CAN CUI</name>
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<sZ>1 aut.</sZ>
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<wicri:noRegion>Sendai 980-8577</wicri:noRegion>
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<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Department of Physics, Zhejiang Sci-Tech University</s1>
<s2>Hangzhou 310018</s2>
<s3>CHN</s3>
<sZ>1 aut.</sZ>
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<country>République populaire de Chine</country>
<wicri:noRegion>Hangzhou 310018</wicri:noRegion>
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<author><name>AN PANG TSAI</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of Multidisciplinary Research for Advanced Materials, Tohoku University</s1>
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<front><div type="abstract" xml:lang="en">In this work, we investigate single-grain 1/1 quasicrystal approximant crystals, grown via the self-flux method, in the Ag-In-Eu system, the structure of which is similar to the 1/1 approximant in the Cd-Eu system. Due to the similarities between the Cd-RE (RE = rare earth) and Ag- In-RE systems, Ag-In-RE can be regarded as a pseudo-binary phase, in which Ag and In replace Cd. Thus, based on the binary phase diagram of Cd-Eu, the growth conditions, including the nominal composition and decanting temperatures, for single-grain Ag-In-Eu 1/1 approximant crystal growth from indium-rich melt-solution were studied. A faceted, centimeter-sized single-grain 1/1 approximant crystal was obtained and characterized using powder X-ray diffraction, scanning electron microscopy and back-reflection Laue X-ray diffraction methods. The results are promising for the synthesis of single-grain approximant crystals in other Ag-In-RE systems.</div>
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<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
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<fA15 i1="01"><s1>Department of Physics, Chuo University</s1>
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<sZ>1 aut.</sZ>
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<fA15 i1="02"><s1>Graduate school of Engineering, Hokkaido University</s1>
<s2>Kita-ku, Tokyo 112-8551</s2>
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<sZ>2 aut.</sZ>
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<fC01 i1="01" l="ENG"><s0>In this work, we investigate single-grain 1/1 quasicrystal approximant crystals, grown via the self-flux method, in the Ag-In-Eu system, the structure of which is similar to the 1/1 approximant in the Cd-Eu system. Due to the similarities between the Cd-RE (RE = rare earth) and Ag- In-RE systems, Ag-In-RE can be regarded as a pseudo-binary phase, in which Ag and In replace Cd. Thus, based on the binary phase diagram of Cd-Eu, the growth conditions, including the nominal composition and decanting temperatures, for single-grain Ag-In-Eu 1/1 approximant crystal growth from indium-rich melt-solution were studied. A faceted, centimeter-sized single-grain 1/1 approximant crystal was obtained and characterized using powder X-ray diffraction, scanning electron microscopy and back-reflection Laue X-ray diffraction methods. The results are promising for the synthesis of single-grain approximant crystals in other Ag-In-RE systems.</s0>
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